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  • New Flow Hydrogenation Reactor

    Posted by PressReleases - May 18, 2011 09:30

     
    ThalesNano are proud to introduce the new H-Cube Pro™, designed to provide higher throughput & enhanced control, a wider temperature range and greater chemistry capabilities.

    As an upgrade to the original H-Cube®, ThalesNano have kept the best features, including: fast reactions, safe high pressure hydrogen generation from water, catalyst cartridges and ease of use; and improved on them dramatically. The H-Cube Pro™ also contains a range of new features including: active cooling for more selective reactions and a new user-friendly interface.

    Advantages include:

    Throughput and Control: With two cells the reactor can generate up to 60 mL/min of hydrogen. Reactants can be hydrogenated at up to 2.0 M (molarity) in concentration with a 70 mm CatCart®. With improved reaction control, users now have the ability to adjust the amount of hydrogen produced at each pressure level between 0 - 60 mL/min.

    Temperature Range: With an improved temperature range of 10-150°C (instead of 25-100°C) users now have the option of selecting lower temperatures as well as performing more difficult reactions at higher temperatures.

    Software: With a new, easy to use interface, users have the ability to monitor reaction parameters in real time, set the duration of a reaction and export data at the end of each reaction. The software uses the inlet and outlet valves to automatically equilibrate the system, run the reaction, and then rinse the lines with solvent.

    For further information on the H-Cube Pro™ please call customer service on 1800 251 799 or email info@johnmorris.com.au



    Tags: hydrogenation reactor, high pressure hydrogen generation, thales nano, thalenano

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    Take The Risk Out Of Ozonolysis

    Posted by PressReleases - January 10, 2011 18:38

    ThalesNano's new flow reactor, the O-Cube has been specifically designed to take the risk out of ozonolysis and other low temperature reactions. The O-Cube enables chemists of any level to safely perform ozonolysis in a laboratory environment while achieving the same results.

     

    The O-Cube works by combining a continuous-flow of substrate with ozone (generated from an in-built ozoniser) at temperatures between room temperature and -20oC. The ozonide reaction intermediate is combined with an oxidative or reductive quench reagent under cooling to generate the required product. The product elutes from the reactor in minutes for quick analysis. The ozone production may be turned off, so that other low temperature reactions may be performed.

     

    The O-Cube has the following advantages

     

    o    Safety – The ozonide is generated and then quenched continuously

    o    Selectivity – The residence time of the substrate in the reactor can be very precisely controlled. This enables the user to target a specific product.

    o    Simplicity - The system automatically controls the delivery of ozone giving true “walk-away” functionality!

     

    For more information on the O-Cube and other ThalesNano products please contact customer service on 1800 251 799 or email info@johnmorris.com.au



    Tags: thalesnano, o-cube, ozonolysis

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    Bench Top Flow Reactor

    Posted by PressReleases - August 16, 2009 04:24

    John Morris Scientific is proud to introduce Thales Nano’s high-temperature, high pressure, bench top flow reactor, the X-Cube. The X-Cube enables complex, difficult and dangerous reactions to be performed easily and safely.

    The X-Cube is optionally supported by an autosampler to perform automated combinatorial synthesis or process optimisation. Its twin reactors are ideal for forming in situ reagents and reacting them in real time. The reactor is easy to control and relieves you from performing demanding and repetitive work.

    Organic reactions are performed in a flow manner, combining the use of temperatures and pressures up to 200oc and 150 bar (2175 psi) respectively and catalyst/reagent cartridges can be combined online.

    The X-Cube can be combined with other X-Cube or H-Cube flow reactors for multistep synthesis.



    Tags: flow reactor

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    Continuous Flow Hydrogenation Reactor

    Posted by PressReleases - August 16, 2009 03:25

    John Morris Scientific would like to introduce Thales Nano’s continuous flow hydrogenation reactor, the H-Cube. The H-Cube utilises water electrolysis to generate hydrogen, making hydrogenation safer, more efficient. Reactions up to 100°C and 100 bar can be used on milligram to multi-gram quantities.

    The H-Cube works by passing the reaction mixture through a flow channel and combining with hydrogen gas. The mixture is heated and pressurized up to 100°C (212°F) and 100 bar (1450 psi) before being passed through a packed catalyst cartridge (CatCart), where the reaction takes place. The disposable cartridge improves safety and usability by reducing the need for further filtration, therefore avoiding subsequent hazards.

    Reaction parameters such as pressure, temperature, flow rate and hydrogen production can be easily controlled and monitored with an easy to use touch screen. The H-Cube is compact, portable and designed to be used within a standard lab fume hood.



    Tags: hydrogenation reactor

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